One of the methods given below is the procedure for the assay of ferrous sulphate as per "I.P.-1996" 

1

FeSO4 + H2O + dil H2So4 × 

Ceric ammonium sulphate and ferroin sulphate

2

NaHCO3 + H2O + H2SO4 × 

ceric ammonium nitrate and ferroin sulphate

3

FeSO4 + H2O + 6N H2SO4 × 

Potassium permanganate solution

4

FeSO4 + H2O + 6N H2SO4 × 

Potassium pemanganate solution an dferroin sulphate

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